Data File D:\\AGLIENT 1260\\DATA\\20150504\\20150504 2015-05-04 08-45-42\\CPK2015-504-09867.DSample Name: CPK2015-504-09867=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 82Acq. Instrument : HY-LCMS-02 Location : P1-B-05Injection Date : 5/4/2015 5:23:42 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150504\\20150504 2015-05-04 08-45-42\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 5/4/2015 1:11:26 PM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20150428\\20150428 2015-04-28 10-32-06\\100-1000MS+3MIN- 1.5_(0.02%FA).M (Sequence Method)Last changed : 5/5/2015 10:56:15 AM by Li Shan(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃ Catalog No : HY-16228 Batch#09867 A-RP-132 Additional Info : Peak(s) manually integrated DAD1 C, Sig=254,4 Ref=off (D:\\AGLIENT...0\\DATA\\20150504\\20150504 2015-05-04 08-45-42\\CPK2015-504-09867.D) 1.447 1.569mAU70060050040030020010000.51 1.7421.522.53min ===================================================================== Area Percent Report ===================================================================== Sorted By : SignalMultiplier : 1.0000Dilution : 1.0000Do not use Multiplier & Dilution Factor with ISTDs Signal 1: DAD1 C, Sig=254,4 Ref=off Peak RetTime Type Width Area Height Area # [min] [min] [mAU*s] [mAU] %----|-------|----|-------|----------|----------|--------| 1 1.447 MF 0.0661 3045.78076 768.16077 98.5972 2 1.569 FM 0.0586 41.97062 11.93528 1.3587 3 1.742 MM 0.0782 1.36329 2.90693e-1 0.0441 Totals : 30.11468 780.38674 ===================================================================== *** End of Report ***HY-LCMS-02 5/5/2015 10:56:16 AM Li Shan(LCMS-02)Page 1 of 1
Data File D:\\AGLIENT 1260\\DATA\\20150504\\20150504 2015-05-04 08-45-42\\CPK2015-504-09867.DSample Name: CPK2015-504-09867=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 82Acq. Instrument : HY-LCMS-02 Location : P1-B-05Injection Date : 5/4/2015 5:23:42 PM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150504\\20150504 2015-05-04 08-45-42\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 5/4/2015 1:11:26 PM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20150428\\20150428 2015-04-28 10-32-06\\100-1000MS+3MIN- 1.5_(0.02%FA).M (Sequence Method)Last changed : 5/5/2015 10:57:40 AM by Li Shan(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃ Catalog No : HY-16228 Batch#09867 A-RP-132 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20150504\\20150504 2015-05-04 08-45-42\\CPK2015-504-09867.D) ES-API, Pos, Sc 1.4391000008000060000400002000000.511.522.53min HY-LCMS-02 5/5/2015 10:58:13 AM Li Shan(LCMS-02)Page 1 of 2
Data File D:\\AGLIENT 1260\\DATA\\20150504\\20150504 2015-05-04 08-45-42\\CPK2015-504-09867.DSample Name: CPK2015-504-09867MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 1.439 569450 408.80 I 407.90 I 204.50 I*MSD1 SPC, time=1.416:1.470 of D:\\AGLIENT 1260\\DATA\\20150504\\20150504 2015-05-04 08-45-42\\CPK2015-504-09867.D ES-API100806040200100200300400500600700800m/z 408.8 204.5 407.9Max: 48776 *** End of Report ***HY-LCMS-02 5/5/2015 10:58:13 AM Li Shan(LCMS-02)Page 2 of 2
