MS Report from Instrument: HY-LCMS-02 File D:\\CHEM32\\1\\DATA\\HEC\\WYF4013-002-1.D Tgt Mass (EZX): Injection Date : 20 Jan 17 10:57 am +0800 Seq. Line : 0 Sample Name : WYF4013-002-1 Location : P2-E-04 Acq. Operator : GZZ_718 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\Chem32\\1\\METHODS\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\METHODS\\1-POS-3MIN-194NM.M Catalog No : HY-10619B Batch#23325 Easy-Access Method: '1-POS-3MIN' Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C*DAD1 B, Sig=214,4 Ref=off mAU200015001.695100050000.5*DAD1 C, Sig=254,4 Ref=off mAU15001250100075050025000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 705000004000003000002000001.33410000000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.522.5min1.7051.2431.1871.3101.69411.2491.2041.3111.2491.522.5min*1.522.5min* RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.20 0.03 3.13 2.86 0.07 321 1.25 0.02 3098.58 2721.47 73.35 321 1.31 0.02 6.31 7.45 0.15 321 1.70 0.05 1116.13 384.11 26.42 291 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.19 0.03 1.45 0.31 0.08 321 1.25 0.02 1700.65 16.08 98.22 321 1.31 0.02 2.67 3.34 0.15 321 1.69 0.06 26.65 9.76 1.54 291HY-LCMS-02 1/20/2017 12:53:51 PM GZZ_718Page 1 of 2
MS Report from Instrument: HY-LCMS-02
Ret. Time: 1.24 <<<< POSITIVE SPECTRA >>>> ES-API Positive800007000060000500003000020000100000200 ES-API Positive1750300400500600700800900m/z40000 161.3 322.2 321.2Ret. Time: 1.33 321.2 663.312501000750 141.3 343.21500 6.4 397.3 397.0 701.5 233.4 233.1 265.3 359.3 588.5 124.1 152.6 174.3 302.72500 327.6 702.3500 663.0 815.5200300400500600700800900m/zRet. Time: 1.70 ES-API Positive6000500040003000 232.1 141.110000 293.2 321.02000 173.1 291.3200300400500600700800900m/zHY-LCMS-02 1/20/2017 12:53:51 PM GZZ_718Page 2 of 2
